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Synthesis of transition metal pnictide nanocrystalline powders by mechanochemical reaction

✍ Scribed by Y.K. Kim; Y.W. Cho

Book ID
116598551
Publisher
Elsevier Science
Year
2005
Tongue
English
Weight
628 KB
Volume
393
Category
Article
ISSN
0925-8388

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The rapid synthesis of nanocrystalline SnO 2 powder using a mechanochemical reaction of SnCl 4 (instead of the widely used tin (II) compounds) with (NH 4 ) 2 CO 3 and the subsequent annealing of the product in air and under an H 2 O/NH 3 atmosphere has been investigated using X-ray powder diffractio