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Synthesis of thiourea-tethered C-glycosyl amino acids via isothiocyanate–amine coupling

✍ Scribed by Barghash, Reham F.; Massi, Alessandro; Dondoni, Alessandro

Book ID
126271295
Publisher
Royal Society of Chemistry
Year
2009
Tongue
English
Weight
317 KB
Volume
7
Category
Article
ISSN
1477-0520

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We report on the photoinduced addition of glycosyl thiols to alkenyl glycines (thiol-ene coupling) to give S-glycosyl amino acids in high yields (53-90%). One of the amino acids thus prepared was used in the construction of a tripeptide via solution phase chemistry. Moreover, a one-pot two-step appr