Synthesis of Thiocarboxamides by the Azolide Method
โ Scribed by Prof. Dr. W. Walter; M. Radke
- Publisher
- John Wiley and Sons
- Year
- 1968
- Tongue
- English
- Weight
- 236 KB
- Volume
- 7
- Category
- Article
- ISSN
- 0044-8249
No coin nor oath required. For personal study only.
โฆ Synopsis
amount of heat, to trifluorothioacetamide (2). On further thiolysis at 40 "C, compound ( 2) is converted into (3) within a period of two to three days.
"C
HzS
CF3CSNH2 + H2S + HC1 --+ CF3CSSH + NH4CI
12)
( 3 )
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