Synthesis of the First Silaamidide
β Scribed by Dr. Gail E. Underiner; Prof. Robert West
- Publisher
- John Wiley and Sons
- Year
- 1990
- Tongue
- English
- Weight
- 263 KB
- Volume
- 29
- Category
- Article
- ISSN
- 0044-8249
No coin nor oath required. For personal study only.
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Second fraclion (catenane isomer 3): Yield 220 m g (17' (dichloroinethane:ethyl acetate 7: 1): m.p > 300 (250 MHL. CD,CI, CD,OD 95.5): 6 = 0 61 (5. 6 H : Ar-CH,). 0.90-2.70 (m. X2H: Ar-C~i,;iiidaliphaticCH2).3.85,3.90(s.6H:OCH,).6.29.6 32(broad.4H:arom. H). 6.79 ) .