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Synthesis of the Benzophenone Fragment of Balanol via an Intramolecular Cyclization Event

✍ Scribed by Denieul, Marie-Pierre; Laursen, Bolette; Hazell, Rita; Skrydstrup, Troels

Book ID
127375442
Publisher
American Chemical Society
Year
2000
Tongue
English
Weight
125 KB
Volume
65
Category
Article
ISSN
0022-3263

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The synthesis of a novel benzodiazocine
The synthesis of a novel benzodiazocine via an intramolecular Staudinger/aza-Wittig cyclization
✍ Ian A O'Neil; Clare L Murray; Andrew J Potter; S.Barret Kalindjian πŸ“‚ Article πŸ“… 1997 πŸ› Elsevier Science 🌐 French βš– 117 KB

The novel pyrrolobenzodiazocine (1) has been prepared by an intramolecular Staudinger/aza Wittig protocol from the precursor azido aldehyde (2) in a remarkable 93% yield. Aldehyde (2) was prepared by coupling protected homoprolinol with 2-azidobenzoic acid followed by deprotection and oxidation.