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SYNTHESIS OF THE 8-PHOSPHABICYCLO[3.2.1]OCTA-2,6-DIENE RING SYSTEM

✍ Scribed by Weissman, Steven A.; Baxter, S. G.


Book ID
121706806
Publisher
Informa UK (Taylor & Francis)
Year
1988
Weight
490 KB
Volume
35
Category
Article
ISSN
0308-664X

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## Differential thermal analysis and differential scanning calorimetry showed that the title compounds decomposed at 240-260°C with release of the fragment RP(0) = CH,. Mass spectral studies also showed this to be a fragmentation pathway. The extruded methylenephosphine oxide could be trapped with