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Synthesis of the 6,7-bis[2-methoxycarbonyl(1,1- dideutero)ethyl] derivative of protoporphyrin IX dimethyl ester

✍ Scribed by Young Key Shim; Ravindra K. Pandey; Kevin M. Smith

Publisher: John Wiley and Sons
Year: 2000
Tongue: English
Weight: 86 KB
Volume: 04
Category: Article
ISSN: 1088-4246
DOI: 10.1002/(sici)1099-1409(200003)4:2<185::aid-jpp179>3.0.co;2-i

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✦ Synopsis

A new total synthesis of a protoporphyrin IX derivative in which the α-methylene protons of the 13,17-(2-methoxycarbonylethyl) substituents are regioselectively deuterated is described. The deuterated porphyrin was obtained using the oxidative cyclization of an a,c-biladiene dihydrobromide.

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