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Synthesis of tertiary amines by selective diborane reduction

โœ Scribed by Russ, Pamela A.; Caress, Edward A.

Book ID
127051035
Publisher
American Chemical Society
Year
1976
Tongue
English
Weight
470 KB
Volume
41
Category
Article
ISSN
0022-3263

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๐Ÿ“œ SIMILAR VOLUMES

Synthesis of Hindered Tertiary Amines by
Synthesis of Hindered Tertiary Amines by a Mild Reductive Amination Procedure.
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Selectivity of tertiary amine oxidations
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Secondary amides activated with a Cbz group can be reduced to their corresponding hemiaminals using lithium borohydride. Hydrogenation then removes the Cbz and hydroxyl groups to produce the related amine. Tertiary amides are not affected.