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Synthesis of substituted 3-nitroso-2,4-pyridinediols for use as analytical reagents

✍ Scribed by Robert E. Leard III; John H. Bedenbaugh; Angela O. Bedenbaugh


Book ID
118284415
Publisher
Journal of Heterocyclic Chemistry
Year
1983
Tongue
English
Weight
363 KB
Volume
20
Category
Article
ISSN
0022-152X

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The reaction of the monolithium derivative of 2-(ckloromethyl)-3-tosylpropene (2) with bmwmethy1trim&y1r dfords the p-8ilyl sldfone 7. which aftex mwhphik lutbstitutiocl followed by fluoride induced @.hnbtion of to8yltrimethylsilrme gives 2-sulnltituted omjllgated dialed L whal cxnnpod 7 reacts firs