Synthesis of Spin Trapping Reagents for Oxygen-Centered Radicals
β Scribed by Kosei Shioji
- Publisher
- John Wiley and Sons
- Year
- 2007
- Weight
- 11 KB
- Volume
- 38
- Category
- Article
- ISSN
- 0931-7597
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β¦ Synopsis
Abstract
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π SIMILAR VOLUMES
This research was supported by the Studienstiftung des deutschen Volkes (stipend for J.K). We thank J. Guin and F. Schleth for conducting some of the hydroamination experiments and K. MΓΌller for preparing the norbornene derivatives.
## Abstract The synthesis of [^15^N]β1,1,3,3βtetrakis(trideuteriomethyl)isoindolinβ2βyloxyl and of some 5βalkyl derivatives have been achieved by standard synthetic routes.^1^ The presence of deuterium improves the sharpness of the signals, and this, together with the incorporation of nitrogenβ15,