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Synthesis of Sphingosine-1-phosphonate and Homosphingosine-1-phosphonate

✍ Scribed by Andrej Tarnowski; Oliver Retz; Thomas Bär; Richard R. Schmidt


Publisher
John Wiley and Sons
Year
2005
Tongue
English
Weight
260 KB
Volume
2005
Category
Article
ISSN
1434-193X

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The synthesis of diethyl Z(1,ldimethylhydrazono)propyl phosphonate (1) and its l-benzoyl derivative (2) is described. The 'H and 13C NMR spectra of 1 and 2 have been completely assigned with the aid of two-dimensional 'H-"C correlation NMR spectroscopy. Spectral data for ethyl a-benzoyl-/J-(l,ldimet