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Synthesis of some cyclopentenones and crystal structure of 4-hydroxy-3,4-bis(4-methoxyphenyl)-5,5-dimethyl-2-cyclopenten-1-one

✍ Scribed by Katayoun Marjani; Mohsen Mousavi; Omid Arazi; Akram Ashouri; Samira Bourghani; Mohammad Rajabi

Publisher
Springer Vienna
Year
2009
Tongue
English
Weight
313 KB
Volume
140
Category
Article
ISSN
0026-9247

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The title compound (C 15 H 12 N 3 OSCl) crystallizes in the monoclinic space group P2 1 /n with a = 11.211( 3), b = 8.106(2), c = 17.494(4) Γ…, Ξ² = 104.49(2)ΒΊ, V = 1539.2(7) Γ… 3 , Z = 4, D cal = 1.371 Mg/m 3 at T = 293 K. The structure was solved by direct methods and refined by full-matrix least-squ