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Synthesis of some 6-S-heterocyclic derivatives of 1,2:3,4-di-O-isopropylidene-α-D-galactopyranose

✍ Scribed by M. A. Martins Alho; N. B. D'Accorso; I. M. E. Thiel


Book ID
112131626
Publisher
Journal of Heterocyclic Chemistry
Year
1996
Tongue
English
Weight
393 KB
Volume
33
Category
Article
ISSN
0022-152X

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Preparation and crystal and molecular st
✍ Peter Köll; Wolfgang Saak; Siegfried Pohl; Bohumil Steiner; Miroslav Koóš 📂 Article 📅 1994 🏛 Elsevier Science 🌐 English ⚖ 858 KB

The title compound was isolated by several recrystallisations from a 1:l mixture of diastereomers which was obtained in 75% yield from the reaction of 1,2:3,4-di-O-isopropylidene-c~-D-galactopyranose with epichlorohydrin. The absolute configuration of this isomer (30% yield) was established by X-ray