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Synthesis of Reduced Transition-Metal Oxides with Hydroxylamine Hydrochloride

โœ Scribed by Manivannan, V.; Goodenough, J. B.

Book ID
121414711
Publisher
American Chemical Society
Year
1998
Tongue
English
Weight
73 KB
Volume
37
Category
Article
ISSN
0020-1669

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โœ V. Manivannan; R. Tichy; J.B. Goodenough ๐Ÿ“‚ Article ๐Ÿ“… 1999 ๐Ÿ› Elsevier Science ๐ŸŒ English โš– 153 KB

Reduction of ammonium molybdate, (NH 4 ) 6 Mo 7 O 24 '4H 2 O, with hydroxylamine hydrochloride. NH 2 OH'HCl, at ambient temperature in aqueous solutions results in amorphous MoO 3 'nH 2 O oxide. Subsequent heat treatment of this oxide yields Mo 1ุŠ O 2 or a hydrogen molybdenum bronze, H x MoO 3 (x:1)