At the reaction temperatures required (between 120 and 14OOC) the product sublimes and deposits in the cooler part of the apparatus as needle-shaped crystals, often twinned; the vanadium tetrachloride formed as by-product is removed in the stream of chlorine (ca. 4 litersihr). In three hours, 500 mg
β¦ LIBER β¦
Synthesis of Pyrylium Salts with Various Anions
β Scribed by A. Dinculescu; T. S. Balaban; Cristina Popescu; D. Toader; A. T. Balaban
- Publisher
- Wiley (John Wiley & Sons)
- Year
- 2010
- Weight
- 529 KB
- Volume
- 100
- Category
- Article
- ISSN
- 0037-9646
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