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Synthesis of porphyrinylamide and observation of N-methylation-induced trans–cis amide conformational alteration

✍ Scribed by Matsumura, Mio; Tanatani, Aya; Kaneko, Tomoyo; Azumaya, Isao; Masu, Hyuma; Hashizume, Daisuke; Kagechika, Hiroyuki; Muranaka, Atsuya; Uchiyama, Masanobu

Book ID
122149810
Publisher
Elsevier Science
Year
2013
Tongue
French
Weight
763 KB
Volume
69
Category
Article
ISSN
0040-4020

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✍ P. Sohár; F. Fülöp; G. Bernáth 📂 Article 📅 1984 🏛 John Wiley and Sons 🌐 English ⚖ 384 KB

The con6gurations and conformations of cis-and tram-N-methyl-and -N-benzyl-4,5-and -5,6tetramethylenetetrahydm-l,3-o~es were determined by 'H and -C NMR spectroscopy. The cis isomers are conformationally homogeneous, having the hetero atom attached to the cydohexyl ring, in the axial and equatorial