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Synthesis of pentasubstituted 3-hydroxy-1,2-dioxolanes

โœ Scribed by Baumstark, Alfons L.; Vasquez, Pedro C.

Book ID
126399023
Publisher
American Chemical Society
Year
1992
Tongue
English
Weight
406 KB
Volume
57
Category
Article
ISSN
0022-3263

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The reaction of pentasubstituted 3-hydro
The reaction of pentasubstituted 3-hydroxy-1,2-dioxolanes (hemiperketals) with trivalent phosphorus compounds: Synthesis of ฮฒ-hydroxy ketones
โœ Alfons L. Baumstark; Pedro C. Vasquez; Yaxiong Chen ๐Ÿ“‚ Article ๐Ÿ“… 1993 ๐Ÿ› John Wiley and Sons ๐ŸŒ English โš– 400 KB

The reaction of a series of 4,4-dimethyl-3,5,5-(R3, R2, ## RI)-3-hydroxy-I,2-dioxolanes la-d [la (R, with trimethyl phosphite or triphenylphosphine produced the p-hydro.xy ketones, 2a-d [(R,R#70H)CMe2-COR3], and the corresponding phosphoryl compounds in high yield. The reactions were slow (-24 ho