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Synthesis of Partially DeuteratedN-Nitrosamines – New Standards in Tobacco-smoke Analysis

✍ Scribed by Peter Gärtner; Katharina Bica; Christian Einzinger


Publisher
Springer Vienna
Year
2004
Tongue
English
Weight
194 KB
Volume
135
Category
Article
ISSN
0026-9247

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Synthesis of [3,3-D2]4-hydroxy-1-(3-pyri
✍ Jyh-Ming Lin; Shantu Amin; Sharon E. Murphy; Jerome J. Solomon; Stephen S. Hecht 📂 Article 📅 1993 🏛 John Wiley and Sons 🌐 French ⚖ 332 KB

## Abstract The synthesis of [3,3‐D~2~]4‐hydroxy‐1‐(3‐pyridyl)‐1‐butanone ([3,3‐D~2~]HPB), an internal standard for the analysis of hemoglobin and DNA adducts of tobacco‐specific nitrosamines, is reported. 3‐Pyridine carboxaldehyde was converted to 2‐(3‐pyridyl)‐1, 3‐dithiane. This was condensed wi