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Synthesis of O2,2′-cyclo-β-D-arabinofuranosyl- and β-D-arabinofuranosyl-5-fluorocytosine

✍ Scribed by E. I. Kvasyuk; I. A. Mikhailopulo; D. Barwolff; D. Cech

Book ID: 112363517
Publisher: Springer US
Year: 1982
Tongue: English
Weight: 334 KB
Volume: 18
Category: Article
ISSN: 0009-3122
DOI: 10.1007/bf00526095

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The synthesis of t h e title canpound (7) is described. [2-14C] cytosine (I) is treated with an aqueous mixture of sodium bisulfite and sodium sulfate at 8OoC for 30 rnin. The resulting solid is then treated with aqueous sodiun hydroxide and passed through a cation exchange colunn, producing [ Z-14C