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Synthesis of Novel Enantiopure Fluorinated Building Blocks from Acyclic Chiral Allylsilanes.

✍ Scribed by Matthew Tredwell; Kenny Tenza; Ma. Carmen Pacheco; Veronique Gouverneur

Publisher
John Wiley and Sons
Year
2006
Weight
22 KB
Volume
37
Category
Article
ISSN
0931-7597

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✦ Synopsis

Abstract

For Abstract see ChemInform Abstract in Full Text.

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methyl protecting groups (BBr,, CHCI,) then gave l a in 70 % yield. The 'H and 13C NMR spectra of 1 a (in D,O/ NaOD) and of 1 b (in CDC1,) reflect the symmetry of the molecules. The methoxyl groups are magnetically equivalent in 1 b, but in the open-chain triester precursor 2b, two