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Synthesis of new imino derivatives of gossypol

✍ Scribed by A. Kh. Khaitbaev; Kh. A. Aslanov; S. A. Auelbekov; Kh. Kh. Khaitbaev; S. M. Saiitkulov

Publisher
Springer
Year
1994
Tongue
English
Weight
123 KB
Volume
30
Category
Article
ISSN
0009-3130

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JMS 0300 apparatus. ## 1. 1-Isopropyl-2.3-dimethoxybenzene (4a). To a s o h of 3a (Aldrich; I00 g, 0.66 mol) in acetone (1 1) and Me2S04 (192.5 ml, 2.03 mol), K,CO, (280 g, 2.03 mol) was added, and the mixture was refluxed with stirring under N, for 45 h. After addition of H,O (1 I), heating was c