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Synthesis of New [1,2,4]Triazolo and [1,2,4]Oxadiazolo[1,3,4]benzotriazepines.

✍ Scribed by T. El Messaoudi; M. El Messaoudi; T. Zair; A. Hasnaoui; M. Esseffar; J.-P. Lavergne

Publisher: John Wiley and Sons
Year: 2010
Weight: 28 KB
Volume: 33
Category: Article
ISSN: 0931-7597
DOI: 10.1002/chin.200244177

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✦ Synopsis

Abstract

For Abstract see ChemInform Abstract in Full Text.

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## Abstract The reaction of N‐aryl‐C‐ethoxycarbonyl nitrilimines with [1,2,4]triazepin‐3,5‐dithione leads to title compounds. The 1,3‐dipolar cycloaddition is completely peri and regioselective. The preferred orientation of addition is predicted correctly by AM~1~ calculation.