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Synthesis of Naturally Occurring, Conformationally Restricted Oxazole- and Thiazole-Containing Di- and Tripeptide Mimetics

✍ Scribed by Dr. Georgi Videnov; Dipl.-Chem. Dietmar Kaiser; Dipl.-Chem. Christoph Kempter; Prof. Dr. Günther Jung

Book ID: 102727074
Publisher: John Wiley and Sons
Year: 1996
Tongue: English
Weight: 544 KB
Volume: 35
Category: Article
ISSN: 0044-8249
DOI: 10.1002/anie.199615031

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✦ Synopsis

COMMUNICATIONS

4a: 1 (473 mg, 1.8 mmol), 3 (430 mg, 1.8 mmol), and bis(triphenylphosphane1-(ethene)platinum (83 mg, 0.12 mmol, 6.2 mol%) in toluene (15 mL) were heated under reflux for 24 h. Afterwards, the precipitate was isolated by filtration, washed several times with THF and CH,Cl,, and dried in vacuum. Yield: 455 mg (50.6%))

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