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Synthesis of N-(Substituted aryl/cyclohexyl)-N'-[5-bromo-5-nitro-2-oxido-1,3,2-dioxaphosphorinane-2-yl]ureas

✍ Scribed by P. Vasu Govardhana Reddy; Y. Hari Babu; C. Suresh Reddy

Publisher
Journal of Heterocyclic Chemistry
Year
2003
Tongue
English
Weight
27 KB
Volume
40
Category
Article
ISSN
0022-152X

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✦ Synopsis

Abstract

N‐(Substituted aryl/cyclohexyl)‐N'‐[5‐bromo‐5‐nitro‐2‐oxido‐1,3,2‐dioxaphosphorinane‐2‐yl]ureas RR'P(O)NHC(O)NHR' (5) were synthesized by the reactions of 2‐bromo‐2‐nitro‐1,3‐propanediol (4) with chlorides of aryl/cyclohexyl carbamidophosphoric acids (3) in the presence of triethylamine at room temperature. Their ir, ^1^H, ^13^C and ^31^P nmr spectral data are discussed.

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