1 3 e n r i c h e d n -a l k y l c h l o r o s i l a n e s w i t h l a b e l i nc o r p o r a t i o n a t s e l e c t i v e p o s i t i o n s a l o n g t h e a l k y l c h a i n s . Compounds w h i c h w e r e p r e p a r e d w e r e : n -n o n y l t r i c h l o r o s i 1 a n e -1 -' 3 C n -d o d e
Synthesis of n-heptyltrichlorosilane 7-13C for preparation of labeled chromatographic surfaces
✍ Scribed by M. E. Gangoda; R. K. Gilpin
- Publisher
- John Wiley and Sons
- Year
- 1982
- Tongue
- French
- Weight
- 175 KB
- Volume
- 19
- Category
- Article
- ISSN
- 0022-2135
No coin nor oath required. For personal study only.
✦ Synopsis
Abstract
This report describes the synthesis of carbon‐13 labeled n‐heptyltrichlorosilane from ^13^C methyl iodide. The product is labeled at the 7‐position of the alkyl chain in a 24% yield.
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