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Synthesis of methoprene via electroreduction of the thiophene ring

โœ Scribed by A. V. Lozanova; V. P. Gul'tyai; A. N. Karaseva; A. M. Moiseenkov

Book ID
112444451
Publisher
Springer
Year
1983
Tongue
English
Weight
505 KB
Volume
32
Category
Article
ISSN
1573-9171

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Oligomers containing from 2 to 6 thiophene units attached by their 2 and 5 positions were synthesized unambiguously by iodine oxidation of a suitable ate complex obtained by stepwise reactions of 9-BBN with methanol, a 2\_lithiothiophene, boron trifluoride etherate, and a second 2-lithiothiophene. T