Synthesis of lower-valent molybdenum oxides in aqueous solutions by reducing Na2MoO4 with NaBH4
โ Scribed by Tsang, Chi Fo; Manthiram, Arumugam
- Book ID
- 124171153
- Publisher
- Royal Society of Chemistry
- Year
- 1997
- Tongue
- English
- Weight
- 312 KB
- Volume
- 7
- Category
- Article
- ISSN
- 0959-9428
- DOI
- 10.1039/A606389F
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๐ SIMILAR VOLUMES
Reduction of KMnO 4 with KBH 4 in aqueous solutions has been investigated systematically at ambient temperatures as a function of reaction pH and the volume of borohydride. The products are characterized by X-ray diffraction, transmission electron microscopy, atomic absorption spectroscopy, redox ti
Reduction of ammonium molybdate, (NH 4 ) 6 Mo 7 O 24 '4H 2 O, with hydroxylamine hydrochloride. NH 2 OH'HCl, at ambient temperature in aqueous solutions results in amorphous MoO 3 'nH 2 O oxide. Subsequent heat treatment of this oxide yields Mo 1ุ O 2 or a hydrogen molybdenum bronze, H x MoO 3 (x:1)