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Synthesis of leukotrienes labelled with deuterium: [11,12,14,15-2H4]-LTA4 -LTC4, -LTD4 and -LTE4

✍ Scribed by J. P. Lellouche; F. Aubert; J. P. Noel; C. Boullais; J. P. Beaucourt

Publisher: John Wiley and Sons
Year: 1989
Tongue: French
Weight: 277 KB
Volume: 27
Category: Article
ISSN: 0022-2135
DOI: 10.1002/jlcr.2580270415

No coin nor oath required. For personal study only.

✦ Synopsis

Semi-hydrogenation by 02 gas on L i n d l a r c a t a l y s t o f an a c e t y l e n i c precursor l e d t o [ l l , 12,14,15-2H4]-LTA4 methyl e s t e r -Ia.

N u c l e o p h i l i c

opening o f t h e epoxide r i n g by amino t h i o a c i d s afforded a f t e r saponificat i o n t h e corresponding deuterated peptidoleukotrienes LTC4, LTD4 and LTE4.

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