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Synthesis of homoallyl alcohol from 1,4-butanediol over ZrO2 catalyst

✍ Scribed by Naoki Yamamoto; Satoshi Sato; Ryoji Takahashi; Kanichiro Inui

Book ID
119215372
Publisher
Elsevier Science
Year
2005
Tongue
English
Weight
132 KB
Volume
6
Category
Article
ISSN
1566-7367

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Synthesis of 3-buten-1-ol from 1,4-butan
Synthesis of 3-buten-1-ol from 1,4-butanediol over ZrO2 catalyst
✍ Naoki Yamamoto; Satoshi Sato; Ryoji Takahashi; Kanichiro Inui πŸ“‚ Article πŸ“… 2006 πŸ› Elsevier Science 🌐 English βš– 313 KB

Dehydration of 1,4-butanediol was investigated over ZrO 2 at temperatures of 325-375 β€’ C. Modification of ZrO 2 with a small amount of sodium hydroxide greatly enhanced the selectivity to 3-buten-1-ol. Temperature-programmed desorption of adsorbed NH 3 and CO 2 elucidated acidity and basicity of the