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Synthesis of hexakis(aryloxy)benzenes: x-ray analysis of hexakis (phenyloxy) benzene and of the acetonitrile clathrate of hexakis (3,5-dimethylphenyloxy) benzene

✍ Scribed by Christopher J. Gilmore; David D. MacNicol; Anthony Murphy; Marie A. Russell

Publisher: Elsevier Science
Year: 1983
Tongue: French
Weight: 250 KB
Volume: 24
Category: Article
ISSN: 0040-4039
DOI: 10.1016/s0040-4039(00)88154-x

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✦ Synopsis

Hexakis(aryloxy)benzenes (I)-(IV), representatives of a new class of molecule, have been prepared by reaction of hexafluorobenzene with the sodium salt of the appropriate phenol in 1,3-dimethyl-2-imidazolidinone (DMEU) as solvent. X-ray analyses of parent (I) and of the acetonitrile clathrate of (II) are described, a novel edge-on interaction between host and guest being found in the latter.

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