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Synthesis of Functionalized 1H-Indenes via Copper-Catalyzed Arylative Cyclization of Arylalkynes with Aromatic Sulfonyl Chlorides

✍ Scribed by Zeng, Xiaoming; Ilies, Laurean; Nakamura, Eiichi

Book ID: 111886564
Publisher: American Chemical Society
Year: 2011
Tongue: English
Weight: 857 KB
Volume: 133
Category: Article
ISSN: 0002-7863
DOI: 10.1021/ja209300c

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## Abstract 1‐Aryl‐1__H__‐benzotriazole derivatives were synthesized __via__ intramolecular cyclization of easily obtained triazenes, using CuI as the catalyst, DMSO as the solvent, __t‐__BuONa as the base, and 1,10‐phenanthroline as the ligand, in up to 97% yield. The synthesis is regiospecific an