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Synthesis of erythro-ω-aminosphingosine and preparation of an affinity column for sphingosine kinase purification

✍ Scribed by Alan P. Kozikowski; Ding Qingjie; Sarah Spiegel

Book ID
103404618
Publisher
Elsevier Science
Year
1996
Tongue
French
Weight
240 KB
Volume
37
Category
Article
ISSN
0040-4039

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## Abstract A sphingosine‐1‐phosphate (S1P) analogue containing a terminal alkyl chain amino group is synthesized in a few steps via olefin cross‐metathesis of an optically resolved intermediate and subsequent phosphorylation. Regioselective acylation of this intermediate at its N terminus in solut