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Synthesis of Enantiomerically Pure (+)- and (-)-3-Methyl-3-(2-naphthyl)-2H-benzo[e][1,2]thiazine 1,1,4-Triones

✍ Scribed by Liu, Zhao-Peng

Book ID: 111865453
Publisher: Japan Institute of Heterocyclic Chemistry
Year: 2007
Tongue: English
Weight: 194 KB
Volume: 71
Category: Article
ISSN: 0385-5414
DOI: 10.3987/com-07-11084

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## Abstract The reaction of methyl 2‐bromo‐6‐(trifluoromethyl)‐3‐pyridinecarboxylate (1) with methanesulfonamide gave methyl 2‐[(methylsulfonyl)amino]‐6‐(trifluoromethyl)‐3‐pyridine‐carboxylate (2). Alkylation of compound 2 with methyl iodide followed by cyclization of the resulting methyl 2‐[methy