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Synthesis of (dialkylamino)disilanes

✍ Scribed by Wan, Yanjian; Verkade, John G.

Book ID
127369100
Publisher
American Chemical Society
Year
1993
Tongue
English
Weight
525 KB
Volume
32
Category
Article
ISSN
0020-1669

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## Abstract 2‐Chloro and 2‐phenoxy substituted 1,1‐bis(diethylamino)ethylenes (4a and 4c) react with elemental sulfur at room temperature to give the inner salt, bis(diethylamino)carbeniumdithiocarboxylate (1a), in excellent yields with extrusion of hydrogen chloride and phenol, respectively, thus