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Synthesis of deuterium- and tritium-labeled 25,26,26,26,27,27,27-heptafluorocholesterol

✍ Scribed by Xiangdong Su; William K. Wilson; George J. Schroepfer

Publisher
John Wiley and Sons
Year
1999
Tongue
French
Weight
494 KB
Volume
42
Category
Article
ISSN
0022-2135

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X-ray and NMR investigation of 25,27-dihydroxy-26,28-bis(diethoxyphosphoryloxy)-tert-butylcalix[4]arene in the 1,2-alternate conformation
✍ Janusz Lipkowski; Myroslav Vysotsky; Joanna Slowikowska; Vitaly I. Kalchenko; Le πŸ“‚ Article πŸ“… 1998 πŸ› John Wiley and Sons 🌐 English βš– 197 KB

The crystal structure of 25,27-dihydroxy-26,28-bis(diethoxyphosphoryloxy)-tert-butylcalix[4]arene (1) (hexane solvate, 1:1) was determined by x-ray crystallography. The crystal data are P2 1 /n, a = 12.652(1) A ˚, b = 12.564(2) A ˚, c = 18.781(4) A ˚, b = 105.56(1)°, V = 2876.0(8) A ˚3, Z = 2. In th