Synthesis of Derivatives of ω-Isocyanato-α-methylamino, ω-Ureido-α-methylamino, and Nα-Methyl-α, ω-diamino Acids
✍ Scribed by Klaus Burger; Jan Spengler; Lothar Hennig; Rainer Herzschuh; Samy A. Essawy
- Publisher
- Springer Vienna
- Year
- 2000
- Tongue
- English
- Weight
- 154 KB
- Volume
- 131
- Category
- Article
- ISSN
- 0026-9247
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Amino (MAO) and a,o-diamino (DAO) oligoamides were prepared using dodecylamine or I,6 diaminohexane as a chain Iimitator. These were characterized by GPC, 'H-NMR and 13C-NMR; molecular models: N-dodecyldodecanamide and I,6 his dodecylaminohexane; trifluoroacetylation was used to dissolve the oligoam
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Water / α-Nitrocycloalkanones / ω-Nitro acids / Surfactant The reaction of various α-nitrocycloalkanones 1 with of the latter with HCOONH 4 /Pd-C, in methanol, at 80 °C affords ω-amino acids 3. The synthesis of methyl 9-aqueous 0.05 M NaOH, at 80 °C, in the presence of cetyltrimethylammonium chlori