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Synthesis of (carbyne)metal complexes by oxide abstraction from acyl ligands

โœ Scribed by Mayr, Andreas.; McDermott, Gregory A.; Dorries, Alison M.

Book ID
118017167
Publisher
American Chemical Society
Year
1985
Tongue
English
Weight
443 KB
Volume
4
Category
Article
ISSN
0276-7333

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Typical synthesis procedure: Tetraethyldiborane (310 mg, 4.43 mmol hydride)[281 was added to 4b (530 mg, 0.83 mmol) [27] in toluene (20 mL). The mixture was heated to 60ยฐC for 15 min (color change to yellow). After cooling, the solution was concentrated under vacuum and allowed to crystallize at -20