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Synthesis of carbazole by Ru3(CO)12-catalyzed reductive carbonylation of 2-nitrobiphenyl: the crystal and molecular structure of Ru3(μ3-NC6H4-o-C6H5)2(CO)9

✍ Scribed by Corrado Crotti; Sergio Cenini; Angela Bassoli; Bruno Rindone; Francesco Demartin

Publisher
Elsevier Science
Year
1991
Weight
727 KB
Volume
70
Category
Article
ISSN
0304-5102

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The reactions of [Pt3R~6(CO),l(p-H)3(p3-H)] (1) with PMe3 and PPh3 have produced the salts [Pt(PR3)3H]-[Pt3R~6(CO)2,(p3-H)(p-H)2]r 5a and 5d, R = Me and Ph in the yields 9% and 22%, respectively. By contrast the reaction of 1 with PPh, in the presence of Me3N0 has yielded the phosphane-substituted d