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Synthesis of C3N4crystals under high pressure and high temperature

✍ Scribed by Duanwei He; Fuxiang Zhang; Xiangyi Zhang; Ming Zhang; Riping Liu; Yingfan Xu; Wenkui Wang


Publisher
SP Science China Press
Year
1998
Tongue
English
Weight
431 KB
Volume
41
Category
Article
ISSN
1674-7283

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## Abstract The reaction of an __N__‐monosubstituted amidine with a β‐ketoester to afford a pyrimidinone is sluggish at best under normal conditions. We now report that this reaction can be effected in moderate yield under high pressure. Thus, 2,6‐dichloro‐4‐pyridyl‐(__N__‐prop‐2‐ynyl)carboxamidine