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Synthesis of aluminum methylcyclohexylphosphinate and its use as flame retardant for epoxy resin

✍ Scribed by Liu, Jiyan; Chen, Jia; Liu, Xueqing; Sun, Shan; Cai, Shaojun

Book ID
126587837
Publisher
John Wiley and Sons
Year
2012
Tongue
English
Weight
420 KB
Volume
38
Category
Article
ISSN
0308-0501

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## Abstract 10‐Ethyl‐9‐oxa‐10‐phosphaphenanthrene‐10‐oxide (**1**) can be nitrated using acetic anhydride and fuming nitric acid. The nitro group is reduced using palladium on charcoal and hydrogen. These reaction conditions are used for the synthesis of an analogous DOPO‐based diaminic hardener (*