I described a method based on the oxidation of diallyl disulfide with magnesium monoperoxyphthalic salt (MMPP) (1) and tetrabutylammonium hydrogen sulfate (TBHS) as phasetransfer reagent. Because the reaction yield was poor, I studied the phasetransfer process; the results show that, at room tempera
Synthesis of Allicin and Purification by Solid-Phase Extraction
✍ Scribed by Gregorio Cruz-Villalon
- Publisher
- Elsevier Science
- Year
- 2001
- Tongue
- English
- Weight
- 56 KB
- Volume
- 290
- Category
- Article
- ISSN
- 0003-2697
No coin nor oath required. For personal study only.
📜 SIMILAR VOLUMES
## Abstract This paper deals with the use of solid‐phase extraction (SPE) for the extraction and purification of 3‐indolylacetic acid (IAA), the main and most important representative of the plant growth regulators auxins. The procedure is based on the use of C18‐SPE columns in two steps. In the fi
Simple one/two step purification procedures based on the solid-phase extraction technique were effectively exploited to clean up radiolabelled drugs represented by dihydrochloride of [6-3 H]-stobadine and hydrochloride of [4-3 H]-pentacaine, derivatization agents such as 4-nitrobenzoyl chloride or 3