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Synthesis of Alkylidenetriazenes (1,2,3-Triazabutadienes). X-Ray Crystal Structure of 1-Methylthio-3-(α-Morpholino) Benzylidenetriazene

✍ Scribed by Gerrit L'abbé; André Willocx; Jean-Paul Declercq; Gabriel Germain; Maurice van Meerssche


Publisher
Wiley (John Wiley & Sons)
Year
2010
Weight
110 KB
Volume
88
Category
Article
ISSN
0037-9646

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## Abstract 2‐Iodoxybenzenesulfonic acid (in a cyclic tautomeric form of 1‐hydroxy‐1__H__‐1,2,3‐benziodoxathiole 1,3,3‐trioxide), a thia‐analog of 2‐iodoxybenzoic acid (IBX) and a potentially important oxidizing reagent, was prepared by two different pathways: direct oxidation of 2‐iodobenzenesulfo