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Synthesis of Adamantane-Based Trimeric Benzoboroxoles

โœ Scribed by Claes, Dorith; Holzapfel, Malte; Clausen, Nadine; Maison, Wolfgang

Book ID
121227506
Publisher
John Wiley and Sons
Year
2013
Tongue
English
Weight
801 KB
Volume
2013
Category
Article
ISSN
1434-193X

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Synthesis and structure of benzoboroxole
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Benzoboroxoles (S) can be prepared from the readily available o-bromobenzyl alcohols via dilithiation followed by reaction with triisopropyiborate. X-Ray structural analysis of 1-hydroxy-3(IH)-1,2-benzoboroxole (Sa) as well as the results of ab initio molecular orbital calculations indicate a planar