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Synthesis of a radiotracer for studying dopamine uptake sites in vivo using PET: 2β-carbomethoxy-3β-(4-fluorophenyl)-[N-11C-methyl]tropane ([11C]CFT or [11C]WIN-35,428)

✍ Scribed by Robert F. Dannals; John L. Neumeyer; Richard A. Milius; Hayden T. Ravert; Alan A. Wilson; Henry N. Wagner Jr.


Publisher
John Wiley and Sons
Year
1993
Tongue
French
Weight
320 KB
Volume
33
Category
Article
ISSN
0022-2135

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✦ Synopsis


Abstract

2β‐Carbomethoxy‐3β‐(4‐fluorophenyl)‐[N‐^11^C‐methyl]tropane, a potent inhibitor of dopamine transport, was prepared by N‐methylation of the appropriate nor‐methyl precursor in DMF with [^11^C]iodomethane. After derivatization of unreacted precursor with a long chain acyl halide, the radiotracer was purified using reversed phase semipreparative HPLC. The average specific activity was 3065 mCi/μmole (calculated at the end‐of‐synthesis; EOS). The average time of synthesis including formulation was approximately 21 minutes.