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Synthesis of a new adrenal cortex imaging agent 6β-131 I-iodomethyl-19-nor cholest -5(10)-en-3β-ol (NP-59)

✍ Scribed by Garabed P. Basmadjian; Kenneth R. Hetzel; Rodney D. Ice; William H. Beierwaltes


Publisher
John Wiley and Sons
Year
1975
Tongue
French
Weight
250 KB
Volume
11
Category
Article
ISSN
0022-2135

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✦ Synopsis


Abstract

A new adrenal cortex imaging agent. 6β‐^131^ I‐iodomethyl‐19‐norcholest‐5(10)‐en‐3β‐ol (NP‐59)[I] was synthesized by the homallylic rearrangement of 19‐iodocholesterol or directly from cholest‐5‐ene‐3β, 19‐diol‐19‐toluene‐p‐sulfonate via homoallylic rearrangement with the iodide ion as a nucleophile and subsequent exchange with Na^131^I. NP‐59 appears to concentrate 5 times better than 19‐iodocholesterol in the rat adrenal and is currently being evaluated as a possible diagnostic agent in man.