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Synthesis of a new 125I-labeled tyrosine methyl ester conjugate of adenylyl-(2′-5′)-adenylyl-(2′-5′)-[2′,3′-di-O-(2-carboxyethyl)ethylidene]adenosine

✍ Scribed by Evgeny I. Kvasyuk; Tamara I. Kulak; Svetlana M. Shulyakovskaya; Mikhail V. Makarenko; Igor A. Mikhailopulo; Charubala Ramamurthy; Wolfgang Pfleiderer


Publisher
Elsevier Science
Year
1996
Tongue
English
Weight
217 KB
Volume
6
Category
Article
ISSN
0960-894X

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The reaction of 2,3:5,6-di-0-isopropylidene-cu-D-mannofuranose with (3methoxycarbonyl-2-oxopropylidene)triphenylphosphorane, catalysed by benzoic acid in dry benzene, gives methyl 4-(2,3:5,6-di-O-isopropylidene-cr-and -@-mannofuranosyl)-3-oxobutanoate in good yield. These compounds are easily transf