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Synthesis of a macroporous silica-based derivative of pyridine material and its application in separation of palladium

✍ Scribed by Anyun Zhang; Xiaoyu Wang; Zhifang Chai

Publisher
American Institute of Chemical Engineers
Year
2010
Tongue
English
Weight
757 KB
Volume
56
Category
Article
ISSN
0001-1541

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## Abstract A method for the preparation of 3‐(fluoroalkyl)‐substituted 2‐azabutadienes **5** by aza‐Wittig reaction of __N__‐vinylic 3‐(fluoroalkyl)phosphazenes **4** and aldehydes is reported. Thermal 6π‐electrocyclization of these azadienes gives 3‐(fluoroalkyl)‐substituted isoquinolines **6**.