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Synthesis of a 2-acetamido-2-deoxy-α-d-galactopyranosyl analogue of tunicamycin

✍ Scribed by Kaichiro Kominato; Seiichiro Ogawa; Tetsuo Suami

Publisher
Elsevier Science
Year
1988
Tongue
English
Weight
599 KB
Volume
174
Category
Article
ISSN
0008-6215

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Synthetic mucin fragments. Benzyl O-(2-a
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✍ Rexford L. Thomas; Saeed A. Abbas; Khushi L. Matta 📂 Article 📅 1988 🏛 Elsevier Science 🌐 English ⚖ 713 KB

Treatment of benzyl 2-acetamido-2-deoxy-alpha-D-galactopyranoside with 4-methoxybenzaldehyde dimethyl acetal in N,N-dimethylformamide in the presence of 4-toluenesulfonic acid afforded the 4,6-O-(4-methoxybenzylidene) acetal, which was glycosylated with 2,3,4,6-tetra-O-acetyl-alpha-D-galactopyranosy

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In a continuing program for the synthesis of oligosaccharides that occur as part of mutinous glycoconjugates, we previously described\* the synthesis of the disaccharide methyl 3-0-(2-acetamido-2-deoxy-P-D-glucopyranosyl)-a-D-galactopyranoside (1). We have also demonstrated that 1 could be readily