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Synthesis of [9, amino-15N2]adenine and β-2′-deoxy-[9, amino-15N2]adenosine

✍ Scribed by Charles C. Orji; Louis A. Silks III

Publisher
John Wiley and Sons
Year
1996
Tongue
French
Weight
290 KB
Volume
38
Category
Article
ISSN
0022-2135

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✦ Synopsis

~-2'-Deoxy-[9,amino-~~N~Jadenosine has been synthesized in 4 steps from commercially available 5-amino-4,6-dichloropyrimidine and 15NH3.

📜 SIMILAR VOLUMES

The first synthesis of [9, amino-15N2] a
The first synthesis of [9, amino-15N2] adenine and β-2′-deoxy-[9, amino-15N2] adenosine
✍ Charles C. Orji; Louis A. Silks III 📂 Article 📅 1996 🏛 John Wiley and Sons 🌐 French ⚖ 290 KB

~-2'-Deoxy-[9,Amino-~~N~]Adenosine has been constructed in 4 steps from commercially available 5-amino-4,6-dichloropyrirnidine and 15NH3. The reactions have been scaled to provide significant quantities of labeled nucleoside.

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✍ M. Weychert; J. Klimkiewicz; I. Wawer; B.Piekarska-Bartoszewicz; A. Temeriusz 📂 Article 📅 1998 🏛 John Wiley and Sons 🌐 English ⚖ 209 KB

The 15N NMR spectra of a series of derivatives of 2-amino-2-deoxy-b-D-glucopyranose and dipeptides or secondary amines were recorded. In the dipeptide derivatives the chemical shift of nitrogen atom N-1 (linked to sugar) is essentially unchanged and the shifts of nitrogen atoms N-3 and N-6 are deter

Infrared and 1H NMR studies of hydrogen
Infrared and 1H NMR studies of hydrogen bonding in N-(2-amino-2-deoxy-β-D-glucopyranoside)-N′-carbamoyl-L-amino acid esters
✍ Monika Plass; Iwona Wawer; Boguslawa Piekarska-Bartoszewicz; Andrzej Temeriusz 📂 Article 📅 1997 🏛 John Wiley and Sons 🌐 English ⚖ 138 KB

Ureido 2-deoxy-␤-D-glucopyranosides with seven different amino acid ester residues were studied by means of IR and 1 H NMR spectroscopy. The H-D exchange rates increase in the order L-Val <L-Leu <L-Ala < Gly for both NH protons; however, the exchange rate at N-1-H (linked to the glucopyranoside) is