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Synthesis of 8,9-dioxabicyclo[5.2.1]decane derivatives from cyclooctene

✍ Scribed by A.J. Bloodworth; B.P. Leddy

Publisher: Elsevier Science
Year: 1979
Tongue: French
Weight: 216 KB
Volume: 20
Category: Article
ISSN: 0040-4039
DOI: 10.1016/s0040-4039(01)93558-0

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✦ Synopsis

Singlet oxygenation of cyclooctene eves 2-cyclooctenyl hyclropercx-Y5e which afzords isomeric 2, &-l0-dibroso-8,9-dioxabicyclo~.2.1]deoanes on treatient with mercury(I1) trifluoroaoetate then bromine , and yields cis-lo-bromo-8,9-dioxabicyclo[5.2.gdecane on treatment with bromine then silver trifluoroaoetate.

Recently we described the preparation of 8,9-dioxabicycloD.2.1)decane (1) by the peroxymerouration and reduction of 1,4-cyclooctsdiene.'

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